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Ni 6 B 22 O 39 ·H 2 O was synthesized in a high-pressure/high-temperature reaction at 5 GPa/900°C. It crystallizes in the orthorhombic space group  Pmn 2 1  (no. 31) with the lattice parameters  a =7.664(2),  b =8.121(2) and  c =17.402(2) Å. The crystal structure is discussed with regard to the isotypic compounds  M  6 B 22 O 39 ·H 2 O ( M =Fe, Co) and the structurally related phase Cd 6 B 22 O 39 ·H 2 O. Furthermore, the characterization of Ni 6 B 22 O 39 ·H 2 O via X-ray powder diffraction and vibrational spectroscopy is reported.

Ni 6 B 22 O 39 ·H 2 O – extending the field of nickel borates