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A new dinuclear bismuth(III) coordination polymer {[Bi(H 2 O)] 2 (C 7 H 3 NO 4 ) 2 (C 12 H 8 N 2 ) 2 (N 3 ) 2 ·2H 2 O}  n   ( 1 ) containing three types of ligands has been synthesized using a solvothermal method and characterized by infrared (IR) spectroscopy, energy-dispersive X-ray spectroscopy, and X-ray single-crystal structural analysis. The compound can be viewed as a three-dimensional supramolecular network that is constructed by Bi 3+  cations, N 3  −  anions, pyridine-2,5-dicarboxylate (2,5-pdc 2− ), and 1,10-phenanthroline (phen) ligands. Moreover, the luminescence properties, quantum yield, luminescence decay, and thermal stabilities of  1  were also investigated.

Crystal structure and luminescence properties of a new dinuclear bismuth(III) coordination polymer containing three types of ligands