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The stannide Sm 2 Rh 3 Sn 5  was obtained by arc-melting of the elements and subsequent annealing at 1070 K in a silica tube. Sm 2 Rh 3 Sn 5  crystallizes with the orthorhombic Y 2 Rh 3 Sn 5  type structure, space group  Cmc 2 1 ,  Z =4:  a =444.46(8),  b =2636.2(4),  c =718.3(1) pm,  wR =0.0711, 1761  F  2  values and 61 variables. The three crystallographically independent rhodium atoms show tricapped trigonal prismatic coordination by samarium and tin atoms. Sm 2 Rh 3 Sn 5  can be considered as a simple 1:1 intergrowth structure of TiNiSi- and NdRh 2 Sn 4 -related slabs of compositions  SmRhSn  and  SmRh 2 Sn 4  . Temperature dependent magnetic susceptibility data revealed van Vleck type behavior caused by the proximity of the exited  6 H 7/2  state to the  6 H 5/2  ground state of Sm 3+ , and an antiferromagnetic ordering occurs at  T  N =3.5(5) K.

Structure and magnetic properties of Sm 2 Rh 3 Sn 5 – an intergrowth of TiNiSi- and NdRh 2 Sn 4 -related slabs