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The neutral, four-fold protonated pyridine-3,5-dicarbox(3,5-dicarboxylatoanilide) (H 4 L) reacts with Mn(II) salts under hydrothermal conditions to yield a new complex: [Mn 2 (L)(H 2 O) 2 ]·H 2 O ( 1 ), which has been characterized by single crystal X-ray diffraction, infrared spectroscopy, and elemental and thermogravimetric analyses. Complex  1  exhibits a binodal (4,8)-connected 3D framework with  flu  (4 12 .6 12 .8 4 )(4 6 ) 2  topology. The magnetic properties of  1  were investigated.

A Mn(II) coordination polymer from a polycarboxylate-containing ligand: synthesis, structural characterization, and properties