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Single crystals of Sc 2 Pt 9 Si 3  have been obtained from an arc-melted and inductively annealed sample of the starting composition Sc:4Pt:2Si. The Sc 2 Pt 9 Si 3  structure (Tb 2 Pt 9 Ge 3  type, space group  C 2/ c ) was refined from single crystal X-ray diffractometer data:  a =1303.4(1),  b =749.9(1),  c =973.5(1),  β =116.44(1)°,  wR 2=0.0731, 1643  F  2  values and 67 variables. The structure contains three basic coordination polyhedra Sc@Pt 11 , Si1@Pt 8  and Si2@Pt 8  which show a simple condensation pattern avoiding direct Sc–Si and Si–Si bonding.

The platinum-rich scandium silicide Sc 2 Pt 9 Si 3