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A new complex [C(NH 2 ) 3 ] 2 [Mn(N 3 ) 4 ], in which Mn II  cations are alternatively bridged by double  EE  azide-bridges and the [Mn(N 3 ) 4 ] n  2−  chains are separated by guanidinium cation bilayers, has been synthesized and characterized by single crystal X-ray diffraction, infrared (IR) spectroscopy, elemental analyses, and magnetic measurements. Magnetic susceptibility data indicate antiferromagnetic interaction among the Mn II  ions.

Synthesis, crystal structure and magnetic properties of the complex [C(NH 2 ) 3 ] 2 [Mn(N 3 ) 4 ] with a polynuclear azido-bridged chain anion