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Interaction of AgCl with bis(diphenylphosphino)methane (dppm) in THF/MeCN in the presence of K[PF 6 ] or [Et 4 N]Br afforded typical trinuclear cationic trigonal-bipyramidal complexes [Ag 3 ( μ  3 -Cl) 2 ( μ -dppm) 3 ][PF 6 ] ( 1 ) or [Ag 3 ( μ  3 -Br) 2 ( μ -dppm) 3 ][AgBr 2 ] ( 2 ), respectively. Treatment of AgBr with bis(diphenylphosphino)ethane (dppe) in THF/MeCN in the presence of [Et 4 N]Br gave a polymeric complex {[Et 4 N][Ag 2 ( μ -Br) 3 ( μ -dppe)]}  n   ( 3 ) with a dinuclear {Ag 2 ( μ -Br) 3 } core. The reaction of AgCl with dppe or bis(diphenylphosphino)propane (dppp) in THF/MeCN in the presence of [Et 4 N]Cl resulted in the isolation of a dinuclear anionic complex [Et 4 N] 2 [(AgCl 2 ) 2 ( μ -dppe)] ( 4 ) with one  μ -dppe bridge or a dinuclear neutral complex [(AgCl) 2 ( μ -dppp) 2 ] ( 5 ) with two  μ -dppp bridges and a 12-membered ring, respectively. The structures of complexes  1–5  with the bidentate phosphine ligands were determined by single-crystal X-ray diffraction.

zeitschrift für naturforschung b

New adducts of silver(I) halides, Ag X  ( X  = Cl, Br), with bidentate phosphine ligands: syntheses and molecular structures of [Ag 3 ( μ  3 -Cl) 2 ( μ -dppm) 3 ][PF 6 ], [Ag 3 ( μ  3 -Br) 2 ( μ -dppm) 3 ][AgBr 2 ], {[Et 4 N][Ag 2  ( μ -Br) 3 ( μ -dppe)]}  n  , [Et 4 N] 2 [(AgCl 2 ) 2 ( μ -dppe)], and [(AgCl) 2 ( μ -dppp) 2 ]