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Gaseous diffusion of  n -hexane into the reaction mixture of sodium dicyanamide NaN(CN) 2  with 15-crown-5 in tetrahydrofuran leads to a sodium dicyanamide compound [Na(15-crown-5)]N(CN) 2  ( 1 ). Compound  1  exhibits a centrosymmetric dumbbell-like structure constructed by dicyanamide ligands double-bridging [Na(15-crown-5)] +  moieties with a μ-1,5 coordination mode. Solid-state photoluminescence experiments have shown that compound  1  emits violet luminescence, and its possible emission mechanism was investigated in detail based on theoretical calculations.

Synthesis, crystal structure, and photoluminescence of a dumbbell-like sodium dicyanamide compound with 15-crown-5