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A facile, efficient, and practical method for   n  Bu 4 NI-catalyzed direct C–H amination of benzoxazoles with tertiary amines has been developed. The system could be performed in the absence of metal catalyst and only requires  tert -butyl hydroperoxide as oxidant under microwave irradiation. A variety of substituted benzoxazol-2-amines were synthesized with moderate to good yield.

n Bu 4 NI-catalyzed direct amination of benzoxazoles with tertiary amines using TBHP as oxidant under microwave irradiation