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The new compounds LiK[C(CN) 3 ] 2  and Li[C(CN) 3 ]·½ (H 3 C) 2 CO were synthesized and their crystal structures were determined. Li[C(CN) 3 ]·½ (H 3 C) 2 CO crystallizes in the orthorhombic space group  Ima 2 (no. 46) with the cell parameters  a =794.97(14),  b =1165.1(2) and  c =1485.4(3) pm, while LiK[C(CN) 3 ] 2  adopts the monoclinic space group  P 2 1 / c  (no. 14) with the cell parameters  a =1265.7(2),  b =1068.0(2) and  c =778.36(12) pm and the angle  β =95.775(7)°. Single crystals of K[C(CN) 3 ] were also acquired, and the crystal structure was refined more precisely than before corroborating earlier results.

Two lithium tricyanomethanide compounds: syntheses and single-crystal structure determination of LiK[C(CN) 3 ] 2 and Li[C(CN) 3 ]·½ (H 3 C) 2 CO