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The semirigid bipyrazolyl and tripyrazolyl  ligands, namely 1,4-bis((3,5-diphenyl-1 H -pyrazol-4-yl)-methyl)benzene (H 2 L 1 ) and 1,3,5-tris((3,5-diphenyl-1 H -pyrazol-4-yl)methyl)benzene (H 3 L 2 ), and their Cu(I) complexes (Cu 2 L 1 )  n   ( 1 ), Cu 4 (HL 2 ) 2  ( 2 ) have been prepared and structurally characterized. Single-crystal X-ray analysis demonstrates that  1  exhibits a 2D structure featuring cyclic trinuclear Cu 3 pz 3  subunits. Complex  2  is a tetranuclear compound in which the tripyrazolyl ligand is partially deprotonated and acts as a  μ  4  bridge connecting four Cu(I) atoms.

Two copper(I) complexes of bi- (or tri-)pyrazolyl ligands featuring Cu 3 pz 3 or Cu 4 pz 4 motifs