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Two highly unstable copper(I) salts, i. e. copper(I) bisulfate tetraacetonitrile, [Cu(CH 3 CN) 4 ]HSO 4 , and dicopper(I) sulfate octaacetonitrile, [Cu(CH 3 CN) 4 ] 2 SO 4 , and their stable derivatives with 2,9- dimethyl-1,10-phenanthroline (DMPhen) have been prepared in pure form and characterized by elemental, spectral and chemical analysis. Single-crystal X-ray studies of [Cu(CH 3 CN) 4 ]HSO 4  and its derivative [Cu(DMPhen) 2 ]HSO 4  have been carried out. The solution behavior of both of these salts and their derivatives have been investigated using UV/Vis, IR,  63 Cu NMR spectroscopy and molar conductance in a number of non-aqueous solvents. Furthermore, a simple method for the preparation of Cu 2 SO 4  is presented.

zeitschrift für naturforschung b

Preparation, Characterization, X-Ray Structure Determination and Solution Properties of some Novel Copper(I) Bisulfate and Sulfate Salts and Their Stable Derivatives