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Single crystals suitable for X-ray diffraction of ( t Bu 2 P) 3 Ga (monoclinic, space group Cc) were obtained from GaCl 3  and two equivalents of Li[PtBu 2 ] at room temperature in benzene. The phosphanylgallane ( t Bu 2 P) 3 Ga was also produced via a one-pot approach by reaction of GaCl 3  with three or more than three equivalents of Li[PtBu2]. However, treatment of one equivalent of GaCl 3  with one equivalent of Li[PtBu 2 ] and subsequent protolysis yielded [ t Bu 2 PH 2 ][ t Bu 2 P(GaCl 3 ) 2  - Li(Cl 3 Ga) 2 PtBu 2 ]. Single crystals of this phosphonium salt (monoclinic, space group Cc) were obtained from benzene at room temperature.

zeitschrift für naturforschung b

Untersuchungen zur Reaktivität des Lithiumphosphanids Li[PtBu 2 ] gegenüber GaCl 3  / Investigations of the Reactivity of the Lithiumphosphanide Li[PtBu 2 ] towards GaCl 3