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The rare earth-rich compounds RE 15 Rh 5 Cd 2  (RE = La, Ce, Pr, Nd) were synthesized by induction melting of the elements in sealed tantalum tubes and characterized by X-ray powder diffraction. The structure of La 15 Rh 5 Cd 2  was refined from single-crystal diffractometer data: new type, R3m, a = 1016.4(2), c = 4418.7(9) pm, wR2 = 0.0417, 2258 F 2 , 95 variables. Striking structural motifs in the RE 15 Rh 5 Cd 2  intermetallics are rhodium-centered trigonal prisms RE 6 Rh which are condensed via common corners and edges to a complex three-dimensional network which leaves cavities for Cd 4  tetrahedra and RE 6  octahedra. The structural relationship with the recently discovered structure types Gd 4 RhIn and Pr 23 Ir 7 Mg 4  is discussed.

Cd 4 Tetrahedra and Condensed RE 6 Rh Trigonal Prisms as Building Units in the Rare Earth-rich Compounds RE 15 Rh 5 Cd 2 (RE = La, Ce, Pr, Nd)