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A luminescent multilayer film has been fabricated from the polyoxometalate anion α- [PMo 12 O 40 ] 3−  (α-PMo 12 ) and the cation Fuchsin Basic (FB) through an electrostatic layer-by-layer (LbL) self-assembly method and characterized by UV/Vis spectra, atomic force microscopy and X-ray photoelectron spectra. The fluorescence properties of the LbL film have also been investigated. Cyclic voltammetry measurements have demonstrated that the electrochemical properties of the polyoxometalate and FB are maintained in the multilayer film, which exhibits electrocatalytic activity for the reduction of bromate

Fabrication and Characterization of LuminescentMultilayer Films Based on Polyoxometalates and Fuchsin Basic