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Reaction of Au(PPh 3 )Cl with MET-TTF in the presence of air resulted in a new charge-transfer salt [AuCl 2 (DDDT)](MET-TTF) (1, DDDT = 5,6-dihydro-1,4-dithiin-2,3-dithiolate, MET-TTF = bis(methylthio)ethylenedithiotetrathiafulvalene). During the air-induced reaction, the Au(I) is oxidized to Au(III), while two C-S bonds in MET-TTF were cleaved simultaneously. In the crystal the radical cations in 1 are assembled into a 1D structure by intermolecular S・ ・ ・ S, S・ ・ ・C, and C・ ・ ・C contacts.

zeitschrift für naturforschung b

An Air-induced Synthesis of a Salt [AuCl 2 (DDDT)](MET-TTF) (DDDT = 5,6-Dihydro-1,4-dithiin-2,3-dithiolate, MET-TTF = Bis(methylthio)ethylenedithiotetrathiafulvalene)