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[nBu 4 N][nBu 2 SbCl 4 ] (1) is synthesized by reaction of nBu 4 NCl and nBu 2 SbCl 3 . [Et 3 SbMe] 2-  [(MeSbCl 3 ) 2 ] (2) is formed from [Et 3 SbMe]I and Me 2 SbCl 3 . The structures of 1 and 2 were determined by single-crystal X-ray diffractommetry.

Syntheses and Structures of [nBu 4 N][nBu 2 SbCl 4 ] and [Et 3 SbMe] 2 [(MeSbCl 3 ) 2 ]