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A new dissymmetrical oxamidate ligand has been used to construct a metal-organic network. Using this ligand, a novel coordination polymer, namely {[Cu(obea)] 2 Cu・CH 3 OH・H 2 O}n (1) [H 3 obea = N1-(2-carboxyphenyl)-N2-(2-hydroxyethyl)oxalamide] has been synthesized and characterized by single-crystal X-ray analysis. The structure of complex 1 consists of neutral trinuclear complex units. Through syn-anti carboxylate bridges, the complex features a 2D structure with a helical substructure. Its magnetic properties have been investigated.

From a Dissymmetrical Oxamidate Ligand to a 2D Coordination Polymer: Synthesis, Crystal Structure and Magnetic Properties