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The manganese-rich ternary cementite phase Mn 1.8 Fe 1.2 C has been synthesized by a ceramic route in an almost quantitative yield, and the crystal structure refinement on the basis of high-resolution X-ray powder diffraction data using MoK α1  radiation has been performed. The carbon atom is found in a slightly distorted trigonal prism composed of Mn and Fe atoms, with a rather narrow bond length range from 1.95 to 2.09 Å . The magnetic susceptibility data clearly indicate long-range ordering phenomena, in particular dominant antiferromagnetic interactions, as predicted by density-functional theory.

Synthesis, High-resolution Crystal Structure Refinement and Magnetic Properties of the Manganese-rich Cementite-type Mn 1.8 Fe 1.2 C