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Addition of excess hexamethylphosphoric triamide (HMPA) to cis-Fe(CO) 4 (SiCl 3 ) 2  led to the exclusive formation of the new complex [SiCl 3 (HMPA) 3 ] +  [Fe(CO) 4 SiCl 3 ] −  by cleavage of an ironsilicon bond. A reaction mechanism is presented, based on density functional theory calculations

Cleavage of an Iron-Silicon Bond by Hexamethylphosphoric Triamide: Synthesis and Characterization of [SiCl 3 (HMPA) 3 ] + [Fe(CO) 4 SiCl 3 ] –