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Reaction of MoO 2 (S 2 CNMe 2 ) 2  with RuCl 3  ・χH 2 O in acetone at reflux afforded [Ru 2 (S 2 CNMe 2 ) 3 - (μ 3 -S 2 CNMe 2 ) 2 ] 2 [Mo 6 O 19 ]・2CH 3 COCH 3  (1・2CH 3 COCH 3 ) which was characterized by singlecrystal X-ray diffraction to show a dinuclear ruthenium-dithiocarbamate species as cation and hexamolybdate as counter anion. The [Ru 2 (S 2 CNMe 2 )3(μ 3 -S 2 CNMe 2 ) 2 ] +  cation may be considered as a combination of [Ru(S 2 CNMe 2 ) 3 ] with a cis-[Ru(S2CNMe 2 ) 2 ] +  species, and the Lindqvist anion [Mo 6 O 19 ] 2−  is located on an inversion center between two cations. Spectroscopic properties along with the electrochemistry of compound 1・2CH 3 COCH 3  are reported.

Synthesis, Structure and Electrochemistry of [Ru 2 (S 2 CNMe 2 ) 3 (μ3-S 2 CNMe 2 ) 2 ] 2 [Mo 6 O1 9 ] · 2CH 3 COCH 3