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Two thioindates [M(en) 3 ] 0.5 InS 2  [en = ethylenediamine; M = Ni (1), Co (2)] were prepared by the reaction of In 2 S 3 , Ni (or Co) and S under solvothermal conditions, and their crystal structures have been determined. Both compounds are isostructural and crystallize in the orthorhombic space group Cmcm. The crystal structures consist of a new type of 1-D sinusoidal chain, which complements the reported I - III types of 1-D [InQ 2  − ]n (Q = S, Te) anions built from InQ 4  tetrahedra. The band gaps of 3.47 eV for I and 3.31 eV for 2 have been derived from optical absorption spectra.

A New Type of 1-D Thioindates, [M(en) 3 ] 0.5 [InS 2 ] (M = Co, Ni), Synthesized by Solvothermal Reaction