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Reactions of [Et 4 N] 2 [WSe 4 ] with two equivalents of [Cu X ] powder gave trinuclear linear compounds [Et 4 N] 2 [(μ-WSe 4 )(Cu X ) 2 ] ( X  = Cl 1, Br 2). Treatment of 1 or 2 with PPh 3  in CH 2 Cl 2  resulted in the formation of tetranuclear cubane-like compounds (μ 3 - X )(μ 3 -WSe 4 )(CuPPh 3 ) 3  ( X  = Cl 3, Br 4). The structures of the heterobimetallic selenium compounds 1 and 4 ・ MeCN were confirmed by single-crystal X-ray diffraction. The nonlinear optical properties of 1 were investigated at λ = 532 nm with a pulse width of 7 ns

zeitschrift für naturforschung b

Structural Transformation from Trinuclear Linear to Tetranuclear Cubane Heterobimetallic Selenium Compounds. Structure and Optical Linearities of [Et 4 N] 2 [(μ-WSe 4 )(CuCl) 2 ]