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New intermetallic compounds RE 4 TCd (RE = Y, La-Nd, Sm, Gd-Tm, Lu; T = Ni, Pd, Ir, Pt) were synthesized by melting of the elements in sealed tantalum tubes in a highfrequency furnace. They crystallize with the Gd 4 RhIn-type structure, space group F 4̄3m, Z = 16. The four gadolinium compounds were characterized by single crystal X-ray diffractometer data: a = 1361.7(1) pm, wR2 = 0.062, 456 F 2  values, 19 variables for Gd 4 NiCd; a = 1382.1(2) pm, wR2 = 0.077, 451 F 2  values, 19 variables for Gd 4 PdCd; a = 1363.6(2) pm, wR2 = 0.045, 494 F 2  values, 19 variables for Gd 4 IrCd; a = 1379.0(1) pm, wR2 = 0.045, 448 F 2  values, 19 variables for Gd 4 PtCd. The rare earth atoms build up transition metal-centered trigonal prisms which are condensed via common corners and edges, leading to three-dimensional adamantane-related networks. The cadmium atoms form Cd 4  tetrahedra which fill voids left in the prisms’ network.

Rare Earth-rich Cadmium Compounds RE 4 TCd (T = Ni, Pd, Ir, Pt)