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The new intermetallic compounds Sr 2 Pd 2 In and Sr 2 Pt 2 In were synthesized from the elements in sealed tantalum tubes in a water-cooled sample chamber of an induction furnace. Both indides crystallize with the HT-Pr 2 Co 2 Al-type structure: C2/c, a = 1048.7(2), b = 603.5(2), c = 830.6(1) pm, β = 103.68(2)°, wR 2  = 0.0492, 743 F 2  values for Sr 2 Pd 2 In; a = 1026.8(2), b = 599.0(1), c = 830.3(2) pm, β = 103.17(1)°, wR 2  = 0.0666, 885 F 2  values for Sr 2 Pt 2 In with 25 variables per refinement. The shortest interatomic distances occur for the Pd-In (Pt-In) and Pd-Pd (Pt-Pt) contacts. The strontium atoms are embedded in complex three-dimensional polyanionic networks of compositions [Pd 2 In] and [Pt 2 In].

Synthesis and Structure of Sr 2 Pd 2 In and Sr 2 Pt 2 In