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An unusual cerium-containing decaoxotungstate complex, (NH 4 ) 3 [Na 5 (H 2 O) 17 Cl]{[Na(H 2 O) 4 ] 2 - [CeW 10 O 36 ]} · 6H 2 O (1) has been synthesized and characterized by IR, TG, and single crystal X-ray diffraction studies (yellow crystals, orthorhombic, space group Imm2, a = 11.473(2), b = 15.225(3), c = 17.646(7) Å, V = 3082.3(15) °A3, Z = 2, R = 0.046). In this compound, sandwichtype [CeW 10 O 36 ] 9−  clusters are linked by binuclear [Na 2 (H 2 O) 8 ] 2+  units by sharing oxygen atoms into linear chains, which are further extended into a 2D supramolecular network via pentanuclear [Na 5 (H 2 O) 17 Cl] 4+  units by strong hydrogen bonding interactions.

zeitschrift für naturforschung b

A Chain-like Polyoxotungstate Constructed from [CeW 10 O 36 ] 9– , [Na 5 (H 2 O) 17 Cl] 4+ , and [Na 2 (H 2 O) 8 ] 2+  Units: (NH 4 ) 3 [Na 5 (H 2 O) 17 Cl]{[Na(H 2 O) 4 ] 2 [CeW 10 O 36 ]}· 6 H 2 O