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Single crystals of BiCl 3  ·CH 3 C 6 H 5  (1) formed from BiCl 3  and toluene have been analysed by X-ray crystallography (triclinic, P1̄, Z = 4, a = 7.308(2), b = 12.013(3), c = 12.284(2) Å , α = 75.02(2), β = 84.23(2), γ = 88.86(2)°, T = 173(2) K).

The Complex BiCl 3 · CH 3 C 6 H 5