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Single crystals of the isotypic hydrides Ba 2 H 3 X (X = Cl or Br) were obtained by solid-state reactions of Ba, NaCl, NaNH 2  and metallic Na, or Ba, NH4Br and Na, respectively, in sealed, silicajacketed stainless-steel ampoules. The crystal structures of the new compounds were determined by means of single crystal X-ray diffraction. Ba 2 H 3 Cl and Ba 2 H 3 Br crystallize in a stuffed anti CdI 2  structure and adopt the space group P3̄m1 (No. 164) with the lattice parameters a = 443.00(6), c = 723.00(14) pm and a = 444.92(4), c = 754.48(14) pm, respectively. The hydride positions are derived by crystallographic reasoning and with the help of EUTAX calculations. The results are compared with known data for binary and ternary alkaline earth metal hydrides.

Syntheses and Crystal Structures of the New Ternary Barium Halide Hydrides Ba 2 H 3 X (X = Cl or Br)