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In 2 Ti 6 (PO 4 ) 6 [Si 2 O(PO 4 ) 6 ] has been obtained by heating (1100 °C) stoichiometric amounts of In 2 O 3 , SiP 2 O 7 , TiP 2 O 7 , and TiO 2  in air. Colourless crystals of the phosphate-silicophosphate suitable for a single crystal structure investigation have been grown by chemical vapour transport (1000°C → 900°C, mixture of 70 mg PtCl 2  and 3.5 mg TiP as transport agent). In 2 Ti 6 (PO 4 ) 6 [Si 2 O(PO 4 ) 6 ] adopts its own structure type (R3̅ (No. 148), Z = 3, a = 8.4380(10) Å , c = 44.295(1) Å , 1809 independent reflections, 109 variables, R1 = 0.044, wR2 = 0.112).

zeitschrift für naturforschung b

Beiträge zur Kristallchemie und zum thermischen Verhalten von wasserfreien Phosphaten, XXXVII [1]. Synthese, Kristallstruktur und kernresonanzspektroskopische Untersuchung von In 2 Ti 6 (PO 4 ) 6 [Si 2 O(PO 4 ) 6 ] – Eine Hybride aus den NASICON und M 4 [Si 2 O(PO 4 ) 6 ] Strukturtypen / Contributions on Crystal Chemistry and Thermal Behaviour of Anhydrous Phospates, XXXVII [1]. Synthesis, Crystal Structure and Nuclear Magnetic Resonance Investigation of In 2 Ti 6 (PO 4 ) 6 - [Si 2 O(PO 4 ) 6 ] – A Hybride Built from Layers with NASICON and M 4 [Si 2 O(PO 4 ) 6 ] Structures