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The solvent-free title compound  2  ∞ [Fe II {H 3 N + CH 2 CH 2 C(OH)(PO 3 H − )(PO 3 H − )} 2 ] was prepared by hydrothermal synthesis and consists of (4,4)-nets of iron octahedra (as the nodes) linked by corner sharing tetrahedra of the phosphonate groups. These layers are stacked in an ABB’A’ sequence and are connected to give a three-dimensional network by hydrogen bonds between the non-Fe-bridging phosphonate groups. Pamidronate, C 3 H 10 NO 7 P 2  −  is a zwitterion with an overall charge of −1.

[Bis(3-ammonium-1-hydroxypropylidene-1,1-bisphosphonato)iron(II)]: TheFe 2+ Salt ofPamidronate, a Clinically Effective Diphosphonate Ligand