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In the systems TiS 2 /NbS 2 , TiSe 2 /NbSe 2 , NbS 2 /TaS 2  und NbSe 2 /TaSe 2  complete miscibility in the solid state has been observed by powder X-ray investigations. Mixed crystals as well as the binary compounds can be prepared by chemical vapour transport reactions using iodine as transport agent in the temperature gradient 1000→900 °C. The gaseous species TiI 3 (g), TiI 4 (g), NbI 4 (g) and TaI 4 (g) are responsible for the transport effect.

zeitschrift für naturforschung b

Chemischer Transport fester Lösungen, 26 [1]. Untersuchungen zur Mischphasenbildung und zum chemischen Transport in den Systemen TiS 2 /NbS 2 , TiSe 2 /NbSe 2 , NbS 2 /TaS 2  und NbSe 2 /TaSe 2  / Chemical Vapour Transport of Solid Solutions, 26 [1]. Formation of Mixed Phases and Chemical Vapour Transport in the Systems TiS 2 /NbS 2 , TiSe 2 /NbSe 2 , NbS 2 /TaS 2  and NbSe 2 /TaSe 2