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Colourless single crystals of TbPS 4  (a = 10.696(2), c = 19.053(4) Å ) were obtained by reaction of the elements (750 °C; 30 h). The compound crystallizes with the PrPS 4  type structure (I4 1 /acd; Z = 16). The structure consists of isolated PS 4  tetrahedra each surrounded by four Tb 3+  cations. Both crystallographically different Tb 3+  cations are coordinated by eight sulfur atoms which are part of four PS 4  tetrahedra. Orange single crystals of LiEuPS 4  (a = 11.498(2), c = 19.882(4) Å ) were prepared by reaction of Eu and P with Li2S4 (700 Å; 20 h). The crystal structure corresponds to the PrPS 4  type, in which tubes running along [001] are occupied by Li atoms, which are surrounded by four S atoms in strongly distorted tetrahedra. LiS 4  and PS 4  tetrahedra are connected via common edges into alternating chains.

zeitschrift für naturforschung b

Der PrPS 4 -Strukturtyp und eine ”aufgefüllte“ Variante: Die Verbindungen TbPS 4  und LiEuPS 4  / The PrPS 4  Type Structure and a Filled Variant: The Compounds TbPS 4  and LiEuPS 4