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Oxidative-addition of methyl iodide, CH 3 I, to the dinuclear gold amidinate [Au 2 (o-Me 2 -form)2] in THF generates a metal-metal bonded Au(II) product, formulated as [Au 2 (o-Me 2 -form) 2 CH 3 I], in quantitative yield under nitrogen at 0 °C and in absence of light. The product is characterized by  1 H NMR, elemental analysis and preliminary X-ray crystallography.

Oxidative Addition of Methyl Iodide to Dinuclear Gold(I) Amidinate Complex: Schmidbaur’s Breakthrough Reaction Revisited with Amidinates