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4-Iodo-L-phenylalanine gives with the chloro bridged compounds [(Et 3 P)PtCl 2 ]2, [(Et 3 P)PdCl 2 ] 2  and [Cp*IrCl 2 ] 2  the N,O-chelate complexes (L)(Cl)M[NH 2 -C(H)(CH 2 C 6 H 4 I)CO 2 ] (M = Pt, Pd, Ir; L = PEt 3 , Cp* ) (1 - 3). Oxidative addition of N-protected 4-iodo-L-phenylalanine methylester to Pd(dba) 2  in the presence of 2,2’-bipyridyl or of triphenylphosphine affords the p-phenyl metallated amino acids (bipy)(I)Pd[C 6 H 4 CH 2 C(H)(NHR)CO 2 Me] (4,5) and (PPh 3 ) 2  (I)Pd[C 6 H 4 CH 2 C(H)(NHR) CO 2 Me] (6,7). Oxidative addition of the coordinated 4-iodo-Lphenylalaninate in (Et 3 P)(Cl)M[NH 2 C(H)(CH 2 C 6 H 4 I)CO 2 ] to Pd(dba) 2  was also observed.

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Metal Complexes of Biologically Important Ligands, CLVI [1]. Metal Complexes of 4-Iodo-L-phenylalanine. Oxidative Addition of 4-Iodo-L-phenylalanine Ester to Palladium(0)