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The coordination chemistry of the unusual, pyrrole-stabilised thioaldehyde molecules, 3,5-dimethylpyrrole-2-carbothioaldehyde (HSPy MeHMe ) and 3,5-dimethyl-4-ethylpyrrole-2-carbothioaldehyde (HSPy MeEtMe ) has been investigated with nickel, palladium and platinum in the complexes [M(κ 2 - SPy MeRMe ) 2 ] (M = Ni, Pd, Pt; R = H, Et). The structure of the cyclometallated derivative [Pd(η 2 - C,N-C 6 H 4 CH 2 NMe 2 )(κ 2 -SPy MeEtMe )] was determined by X-ray diffraction.

Pyrrole Thioaldehyde Complexes of Nickel, Palladium and Platinum