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The single crystal X-ray diffraction study of [(η 5 -C 5 H 4 SiMe 3 ) 2 LuCl] 2 , prepared from LuCl 3  and Na[C 5 H 4 SiMe 3 ], shows the compound to be a centrosymmetric dimer with two η 5 -bonded cyclopentadienyl rings and two symmetrically bridging chlorine atoms coordinated to each of the two metal centers. The coordination geometry around the lutetium atoms is that of a distorted pseudo tetrahedron. The Lu-C(Cp) distances lie within the narrow range of 2.571 - 2.608 Å . The Lu-Cl bond lengths are 2.639(1) and 2.653(1) Å . The crystal structure shows no significant intermolecular contacts.

Crystal and Molecular Structure of [(η 5 -C 5 H 4 SiMe 3 ) 2 LuCl] 2 : A Precursor for the Production of Lu 2 O 3 Films