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In contrast to the tetrachlorodigermane (tBu 3 Si)Cl 2 Ge-GeCl 2 (SitBu 3 ), the cis,transcyclotrigermane (tBu 3 SiGeCl) 3  is sensitive to oxygen. Its treatment with O 2  at ambient temperature leads to the trigermoxetane (tBu 3 Si) 3 Ge 3 Cl 3 O. According to an X-ray structure analysis of single crystals consisting of cocrystallized (tBu 3 Si) 3 Ge 3 Cl 3 O and (tBu 3 Si)Cl 2 Ge-GeCl 2 (SitBu 3 ) the trigermaoxetane contains an almost planar Ge 3 O-ring while the tetrachlorodigermane (tBu 3 Si)Cl 2 Ge- GeCl 2 (SitBu 3 ) possesses a Si-Ge-Ge-Si chain which is exactly all trans

Supersilylated Tetrachlorodigermane (tBu 3 Si)Cl 2 GeGeCl 2 (SitBu 3 ) and Trigermoxetane (tBu 3 Si) 3 Ge 3 Cl 3 O