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By reaction of chloro bridged halfsandwich complexes with silver salts and subsequent addition of isocyanocarboxylic acid esters the isocyanide complexes [(arene)M(CNCHR 1 CO 2 R 2 ) 3 ] 2+ (X − ) 2  (arene = C 6 Me 6 , p-cymene, M = Ru; arene = C 5 Me 5 , M = Rh, Ir), (R 1  = H, Me, CHMe 2 , CH 2 Ph, X = BF 4 , CF 3  SO 3 ) were prepared and characterized. The structure of [(C 5 Me 5 ) Ir(CNCH 2 CO 2 Et) 3 ] 2+ (CF 3 SO 3  − ) 2  was determined by X-ray structure analysis.

zeitschrift für naturforschung b

Tris(2-isocyanocarbonsäureester)-Halbsandwich-Komplexe [(Aren)M(CNCHR 1 CO 2 R 2 ) 3 ] 2+  (M = Ru, Rh, Ir) / Tris(2-isocyanocarboxylic Acid Ester) – Halfsandwich Complexes [(arene)M(CNCHR 1 CO 2 R 2 ) 3 ] 2+  (M = Ru, Rh, Ir)