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The octadentate ligand [N(CH 2 CH 2 NH 2 )(CH 2 CH 2 CH 2 OH)(CH 2 CH 2 S)] 2 CH 2 , (NNOS-232) 2 CH 2 , was synthesized accidentally by the reaction of the unsymmetrically substituted tripod [N(CH 2 CH 2 NH 2 )(CH 2 CH 2 CH 2 OH)(CH 2 CH 2 SH)], NNOS-232, with dichloromethane in the presence of aluminum hydroxide. Ligand (NNOS-232) 2 CH 2  was reacted with zinc bis(perchlorate) hexahydrate to yield the complex [Zn((NNOS-232) 2 CH 2 )](ClO 4 ) 2  1 exhibiting a distorted octahedrally coordinated zinc atom in an N 4 S 2  coordination environment, as shown by an X-ray diffraction study.

A Novel Methylene Dithioether as a Ligand: Synthesis and Molecular Structure of a Zinc(II) Complex with N 4 S 2 Coordination Environment