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The imidovanadium(III) complexes [ t BuN=VCp(PR 3 ) 2 ], [ t BuN=VCp{P(OR) 3 } 2 ] and [tBuN= VCp(CO) 2 ] have been prepared starting from  t BuN=VCpCl 2  by reductive dehalogenation with magnesium. The reaction of [ t BuN=VCp(PMe 3 ) 2 ] (2a) with carbon monoxide, alkynes, alkenes, tert-butylphosphaalkyne, nitriles, ketones and carbon disulfide furnished the complexes [ t BuN=VCp(PMe 3 ) (L)], while the vanadium(V) compound  t BuN=VCp(O 2 C 2 Ph 2 ) is formed with benzil. All vanadium(III) complexes obtained are diamagnetic (d 2 , low-spin configuration) and have been characterized by spectroscopic methods (MS;  1 H,  13 C,  31 P,  51 V NMR).

zeitschrift für naturforschung b

Darstellung und  51 V-NMR-spektroskopische Untersuchungen von η 5 -Cyclopentadienyl-tert-butylimidovanadium(III)-Komplexen mit σ-Donator, π-Akzeptor-Liganden / Synthesis and  51 V NMR Spectroscopic Studies of η 5  -Cyclopentadienyl-tert-butylimidovanadium( III) Complexes with σ -Donor, π -Acceptor Ligands