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The red title compound was synthesized by the metathesis reaction of [FeCl 2 (dppe)] (dppe = Ph 2 PCH 2 ) 2 PPh 2 ) and NaS-tBu in THF. The X-ray structure analysis revealed a dinuclear complex with two iron(II) centers coordinated in a distorted tetrahedral fashion by two bridging thiolates, one bridging dppe molecule and one terminal chloro ligand.

Synthesis and Molecular Structure of [Fe 2 Cl 2 (μ-S-tBu) 2 (η 1 -η 1 -μ-dppe)] (dppe = Ph 2 P(CH 2 ) 2 PPh 2 )