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Treatment of 1-methylimidazol-2-yl lithium with Cp 2 Zr(Cl)CH 3  (6) gave the corresponding methyl(1-methyl-2-imidazolyl)zirconocene complex 7. Treatment of 7 with B(C 6 F 5 ) 3  (8) led to selective methyl abstraction. The resulting (imidazolyl)zirconocene cation 9 dimerized under the reaction conditions to yield the dinuclear imidazolyl bridged bis(zirconocene) dication complex 10 that was structurally characterized by X-ray diffraction and by DFT calculations.

Formation of a Doubly C,N-Bridged Six-Membered Metallacyclic Bis[(2-imidazolyl)zirconocene] Dication