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The reaction of Cp*V(CO) 4  (1) with molecular oxygen in diluted pentane solution leads to a tetrameric dioxide, [Cp*V(O)(μ-O)] 4  (2), which is a precursor of the octanuclear aggregate Cp* 6 V 8 O 17  (3). The molecular structures of 1 and 2 have been determined by X-ray crystallography.

zeitschrift für naturforschung b

Decarbonylation of Pentamethylcyclopentadienyl Tetracarbonylvanadium, Cp*V(CO) 4 , in the Presence of Oxygen. The X-Ray Crystal Structure Analyses of Cp*V(CO) 4  and [Cp*V(O)(μ-O)] 4