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Both title compounds were found to crystallize from the system ScCl 3  / K 2 CO 3  / H 2 O and their crystal structures have been determined: K 5 [Sc(CO 3 ) 4 ] ∙ 5 H 2 O is monoclinic, space group P2 1 /n with a = 883,06(13), b = 1826,2(2), c = 1113,2(2) pm, β = 93,28(2)°, V = 1792,3(4) ∙ 10 6  pm 3 , Z = 4), while K 7 [Sc(CO 3 ) 4 ]CO 3  ∙ 9 H 2 O is monoclinic, space group C2 with a = 1395,98(13), b = 1081,35(7), c = 3378,1(4) pm, β = 93,76(1)°, V EZ  = 5088,4(8) ∙ 10 6  pm 3 , Z = 8). Both compounds contain discrete [Sc(CO 3 ) 4 ] anions.

zeitschrift für naturforschung b

Untersuchungen im System ScCl 3  / K 2 CO 3  / H 2 O: Synthese und Kristallstrukturen von K 5 [Sc(CO 3 ) 4 ] · 5 H 2 O und K 7 [Sc(CO 3 ) 4 ]CO 3  · 9 H 2 O / Investigations on the System ScCl 3  / K 2 CO 3  / H 2 O: Synthesis and Crystal Structures of K 5 [Sc(CO 3 ) 4 ] · 5 H 2 O and K 7 [Sc(CO 3 ) 4 ] CO 3  · 9 H 2 O