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Thiotrithiazyl iododichloride, S 4 N 3 ICl 2 , has been synthesized from molecular S 4 N 4  and liquid ICl and structurally characterized by an X-ray Rietveld refinement. S 4 N 3 ICl 2  crystallizes in the monoclinic system (P2 1 /c, a = 611.548(7), b = 877.336(8), c = 1770.12(2) pm, β = 92.3357(7)°, Z = 4), follows the crystal-chemical motif (S 4 N 3  + )(ClICl − ), and is thus isotypic with (S 4 N 3  +  )(Br 3  −  ). The crystal structure contains a planar S 4 N 3  +  ring and a linear ClICl −  unit.

Synthesis and X-Ray Crystal Structure Determination of Thiotrithiazyl Iododichloride, S 4 N 3 ICl 2