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N-Methylisatin N(4)-dimethylthiosemicarbazone, HMIs4DM, prepared by condensation of N-methylisatin and N(4)-dimethylthiosemicarbazide crystallizes in the orthorhombic space group Pbc2 1 , with a = 7.539(1), b = 11.566(4), c = 29.320(1) Å, V = 2556.6(9) Å 3  and Z = 8. Cadmium metal was oxidized in the presence of HMIs4DM in an acetonitrile solution, which produced a complex of the formula [Cd(MIs4DM) 2 ]. [Cd(MIs4DM) 2 ] crystallizes in the orthorhombic space group Pbcn with a = 15.529(5), b = 10.672(4), c = 16.247(3) Å , V = 2692.7(14) Å 3  and Z = 8. [Cd(MIs4DM) 2 ] is symmetrical with two identical MIs4DM ligands that are at an angle of about 80°.

Structure of N-Methylisatin N(4)-Dimethylthiosemicarbazone and its Electrochemically Synthesized 6-Coordinate Cadmium(II) Complex