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Pseudobinary cyanides of monovalent and divalent metals were synthesized, and X-ray and Raman data of the cyanides were measured. Single crystal X-ray structure analyses were performed on Zn(CN) 2  (Pn3̄m (No. 224), a = 591.32(7) pm), Hg(CN) 2  (I4̄2d (No. 122), a = 969.22(14) and c = 890,15(18) pm) and for the first time on AgCN (I4̄2d (No. 166), a = 600.58(8) and c = 526.28(11) pm). The data are compared with literature data. The reaction of TlF and NaCN in 25% aqueous ammonia solution in air led to Tl 5 (CO 3 ) 2 (CN) which was characterized by X-ray (Cmca (No. 64), 1468.1(3), 1171.6(2) and 1266.0(3) pm) and Raman spectroscopy.

X-Ray and Raman Investigations on Cyanides ofMono- and DivalentMetals and Synthesis, Crystal Structure and Raman Spectrum of Tl 5 (CO 3 ) 2 (CN)