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The article reports the first transitionmetal complex of methanesulfonylhydrazine, a molecule known for important pharmacological and chemical applications. The complex [ZnCl 2 (MSH) 2 ], MSH = CH 3 SO 2 NHNH 2 , has been synthesized and its structure characterized by means of X-ray analysis. The coordination geometry is pseudo-tetrahedral and the ligand MSH adopts a conformation that was found by previous ab initio calculations to be a transition state and not a stationary point for the free ligand.

Synthesis and Structure of the First Transition Metal Complex with Methanesulfonylhydrazine as a Ligand