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Syntheses of the homoleptic trimethylsilanolato complexes V(OSiMe 3 ) 3  and V(OSiMe 3 ) 4  are described. The thiovanadium(V)compound VS(OSiPh 3 ) 3  (11) is formed from [V(OSiPh 3 ) 3 - (THF) 2 ] upon oxidation with elemental sulfur; 11 has been characterized by  51 V NMR spectroscopy.

Silanolato-Komplexe von Vanadium (III, IV) / Silanolato Complexes of Vanadium (III, IV)