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Tetrabutylammonium carbonyltribromoplatinate(II) [(C 4 H 9 ) 4 N][PtBr 3 (CO)] crystallises in the monoclinic system in the space group P2 1 /n with a = 1487.84(13), b = 897.41(8), c = 1849.6(2) pm, β = 106.558(2)° and four formula units per unit cell. The [PtBr 3  (CO)] -  anion is symmetrical (C 2v ) and almost planar with Pt-Br bond lengths of 242.40(12) pm (trans to CO), 243.25(10) pm and 242.99(9) pm (trans to Br), and a Pt-C bond length of 185.6(11) pm.

Crystal Structure of Tetrabutylammonium Carbonyltribromoplatinate(II) [(C 4 H 9 ) 4 N][PtBr 3 (CO)]